Synthesis of Isopentyl Acetate

Jane Eunice Agapito, Denmarc L. Aranas*, Limuel Joseph Versus. Bacani, and Steven Arthur Baluyot

Examination of Hydrocarbons

Department of Biology, College or university of Santo Tomas, Manila, Philippines


In this research we performed parallel chemical substance test approach to identify a mysterious. The reflux setup was used to prevent evaporation in mixing the reactants in an inert solvent with its boiling level. Another highlight of this try things out is the liquid-liquid extraction where a solution containing a mixture of ingredients is shaken with a second solvent that is immiscible with it. The percent yield calculated was 59. 23%. The characteristics of the synthesized ester were water, oily, and it had something veryyyy sexy smell. Intro

Artificial flavoring is commonly used in the food we eat today. For example , fresh fruit flavoring can be described as chemical mix that imitates a natural taste as regarding banana flavor from the synthesis of isoamyl acetate. Ester is the useful group, which can be responsible for the distinctive odor and flavor that artificial fruit flavoring has. Esters are produced from carboxylic stomach acids. A carboxylic acid contains the –COOH group, and in a great ester the hydrogen from this group is usually replaced with a hydrocarbon group of some kind. This may be an alkyl group just like methyl or perhaps ethyl, or perhaps one containing a benzene ring like phenyl[1].

Esters happen to be widespread in nature. Little esters, in combination with other unstable compounds, generate the nice aroma of fruits. It truly is amazing that so many fragrances and tastes can be made by simply changing the number of carbons and hydrogens in the ester.

Any organic flavor is commonly quite complex, with many or hundreds of chemicals communicating to create the taste/smell. Nonetheless it turns out that numerous flavors -- particularly fruit flavors -- have just one or a few prominent chemical components that carry the bulk of the taste/smell signal. Several chemicals are esters [2].

This kind of experiment attempts to produce a great ester simply by refluxing liquor with acetic anhydride and an acid catalyst. The objectives in the experiment in order to prepare isoamyl acetate using Fischer esterification and to identify the % yield in the reaction. The preparation of food flavors are done with the use of Fischer response or Fischer esterification. It really is through refluxing of carboxylic acid and an liquor in the presence of an acidity catalyst. The reaction was first described by Emil Fischer and Arthur Speier in 1895 [3]. Results and discussion

In the Pre-laboratory discussion, the Constraining reactant was calculated among isoamyl alcohol and acetic anhydride to find the value of the theoretical deliver. CH3 U O CH3 O To


installment payments on your 5 cubic centimeters

2 . 6 ml



ПЃ= 1 ) 0820 g/ml

ПЃ = 0. 8092 g/ml

Isoamyl alcohol (A) Acetic anhydride (B) Isoamyl acetate (C) Acetic acid

mol C = 2 . five ml A x (0. 8092 g/ml) x 1mol A/88g A x you mol C/1mol A sama dengan 0. 0230 mol C

mol C = installment payments on your 6 ml B x (1. 0820 g/ml) back button 1mol B/102. 1g N x 1 mol C/1mol B = 0. 0276 mol C

The Limiting reactant is usually isoamyl alcohol with zero. 0230mol. After that, we worked out the theoretical yield making use of the mole of isoamyl alcohol.

Theoretical yield = 0. 0230 mol A back button (1 mol C / 1 mol A) x (130. a couple of g C / you mol C) =

3. 00 g isoamyl acetate

This implies that at least a few. 00 g isoamyl acetate will be obtained in the test. The ester that was collected in the vial was weighed in the analytical stability with the reading 23. 3533 g and subtracting it with the fat of the vacant vial which is 21. 5764 g we now got the actual yield of 1. 7769 g.

Calculation intended for the percent yield:


Table one particular

% Yield = (Actual yield as well as Theoretical yield) x 100 %

% Yield = (1. 7769 g / 3. 00g) x completely = fifty nine. 23%

The results are shown in Desk 1 . The physical real estate that the man-made fruit flavor possess...

Referrals: [1]Clark, M. (2004). An introduction to Esters. Chemguide. Gathered July 6th, 2013 coming from:

[2]Recovered July 6th, 2013 from:

[3]Lehman, J. (2001). Operational organic and natural chemistry (3rd Ed. ). Prentice hall: USA.

[4]Kilway, K., & Drew, A. (2007). Fisher esterification: Preparing of clown oil. University or college of Missouri: Kansas.

[5]Aberdeen, S. (2011). Chemistry and reflux. eHow. Retrieved This summer 6, 2013 from:

[6]Retrieved This summer 6, 2013 from:

[7] Fischer esterification. Organic Chemistry. org. Retrieved September 6, 2013 from

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